Chiang Mai Journal of Science

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Microscopy Investigation of Streblus asper Lour. Leaves-derived SiO2/C with Polypyrrole Nanocomposites as Sustainable Anode Materials for Lithium-ion Batteries

Kittiched Khunpakdee, Thanapat Autthawong, Natthakan Ratsameetammajak and Thapanee Sarakonsri
* Author for corresponding; e-mail address: thapanee.s@cmu.ac.th
Volume: Vol.51 No.6 (November 2024)
Research Article
DOI: https://doi.org/10.12982/CMJS.2024.099
Received: 7 August 2024, Revised: 17 October 2024, Accepted: 17 October 2024, Published: 29 November 2024

Citation: Khunpakdee K., Autthawong T., Ratsameetammajak N. and Sarakonsri T., Microscopy investigation of Streblus asper Lour. leaves-derived SiO2/C with polypyrrole nanocomposites as sustainable anode materials for lithium-ion batteries, Chiang Mai Journal of Science, 2024; 51(6): e2024099. DOI 10.12982/CMJS.2024.099.

Abstract

     Lithium-ion batteries (LIBs) are chemically reactive rechargeable energy storages. Silica (SiO2) is one of the most popular alternative materials to replace graphite as an anode material in LIBs due to its higher specific capacity, non-toxicity, and natural resources. Streblus asper Lour. (Khoi) is widely grown in Southeast Asia and contains high SiO2 and SiO2/C levels in its leaves. In order to overcome the volume change issue of Si-based materials and enhance cycle stability, carbon (C) and polypyrrole (PPy) were utilized to reinforce the SiO2 structure during the lithiation/delithiation process. X-ray diffraction (XRD) was utilized to investigate the SiO2, C, and PPy amorphous phases of the synthesized products. Fourier transform infrared spectroscopy (FT-IR), which confirmed the formation of PPy in composites. The scanning electron microscopy (SEM) images revealed different morphologies of SiO2 aggregates, SiO2/C with plate layers, the network structure of PPy and in the composites with PPy. Transmission electron microscopy (TEM) revealed the aggregation of nano-sized SiO2, SAED phase confirmation, and demonstrated the coating of PPy on SiO2/C (KSCPy composites), indicating the presence of C and PPy as supporters. In addition, the performance of synthesized composites as anodes was investigated by assembling them into half-coin cells and performing electrochemical tests. Khoi-SiO2/C/PPy (KSCPy) obtained a specific capacity of 497.9 mA g−1 for 400 cycles at 0.1 A g−1 and the lowest charge transfer resistance. Furthermore, these materials have the potential to be used as sustainable anode materials in LIBs due to their use of natural materials, a non-toxic synthesis method, and C and PPy as both support materials and conductive polymers, which can enhance electrical performance as anode materials.

Keywords: biomass, silica, carbon, nanocomposites, conductive polymer, anode materials, lithium-ion batteries

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Pidchaporn Panyoyai, Chulin Likasiri*, Pachara Tinamas and Wetchayan Rangsri

Vol.40 No.3 (JULY 2013)
Research Article View: 919 Download: 345
Production of Probiotics Streptomyces Biomass from Starchy Wastewater
page: 294 - 298

Suteera Srisamai, Phonlawat Srikhampa, and Wasu Pathom-aree*

Vol.40 No.2 (APRIL 2013)
Research Article View: 1,325 Download: 273
Effects of Reprocessing on the Structure and Properties of Polycarbonate/Multi-Walled Carbon Nanotube Based Electrostatic Dissipative Composites
page: 261 - 273

Darunee Aussawasathien*, Natcha Prakymoramas, and Dumrong Thanomjitr

Vol.40 No.2 (APRIL 2013)
Research Article View: 911 Download: 279
SUZ-4 Zeolite Synthesis Derived from Rice Husk Ash
page: 109 - 116

Napapan Jaroonvechatam [a,c], Pakkarada Sansuksom [a], Patcharin Worathanakul [b] and Paisan Kongkac

Vol.40 No.1 (JANUARY 2013)
Research Article View: 949 Download: 486
Preparation and Performance Test of a Simplified Screen-Printed Carbon Electrode for Use as a Chronoamperometric Transducer in Genosensor
page: 610 - 622

Low Kim Fatt [a], Kritsanaporn Chuenrangsikul [b], Patsamon Rijiravanich [b], Werasak Surareungchai

Vol.39 No.4 (OCTOBER 2012)
Research Article View: 836 Download: 235
Preparation and Properties of Woven Carbon Fiber Mat-Epoxy Composites Containing Dispersed Base-Functionalized Multi-Walled Carbon Nanotubes
page: 524 - 539

Darunee Aussawasathien*, Chanpen Teerawattananon

Vol.39 No.3 (JULY 2012)
Research Article View: 794 Download: 263
Biological Activities of Supercritical Carbon Dioxide Fluid (scCO2) Extracts from Medicainal Flowers
page: 84 - 96

Bang-on Kietthanakorn, Warintorn Ruksiriwanich, Worapaka Manosroi, Jiradej Manosroi and Araya Manosr

Vol.39 No.1 (JANUARY 2012)
Research Article View: 882 Download: 629
Fluid Flow Induced Shear Stress Affects Cell Growth and Total Flavone Production by Phellinus igniarius in Stirred-Tank Bioreactor
page: 69 - 75

Hu Zhu, Wei Liu, Baozhen Tian and Shuaisshuai Zhang

Vol.39 No.1 (JANUARY 2012)
Research Article View: 912 Download: 272
Post-treatment by Sodium Silicate after Zinc Phosphating on Cold-Rolled Steel
page: 30 - 40

Supunsa Dech-oup, Sirinee Thaiwatthana and Torranin Chairaungsri

Vol.39 No.1 (JANUARY 2012)
Research Article View: 889 Download: 301
Preparing Activated Carbon from Palm Shell for Biodiesel Fuel Production
page: 572 - 578

Achanai Buasri, Nattawut Chaiyut and Chaiwut Nakweang

Vol.38 No.4 (OCTOBER 2011)
Research Article View: 897 Download: 347
A Comparative Study of the Cure Characteristics, Processability, Mechanical Properties, Heat Aging, and Morphology of Rice Husk Ash and Silica Fillers in Natural Rubber Compounds
page: 265 - 273

Wanvimon Arayapranee* [a] and Garry L. Rempel [b]

Vol.31 No.3 September 2004
Research Article View: 1,002 Download: 360
Synthesis and Applications of Silica Supported Dichlorotriazine (Si-DCT) in Nucleophilic Scavenging
page: 203 - 209

Mookda Pattarawarapan* and Sunantanee Singhatana

Vol.33 No.2 (MAY 2006)
Research Article View: 842 Download: 301
Adhesion of Borosilicate Glass and Fe-Ni-Co Alloy Joined by Direct Fusion
page: 191 - 202

Waraporn Piyavit [a], Chutimun Chanmuang [a], Manat Jaimasit [b], Warrapong Thiemsorn [b], Akadech

Vol.33 No.2 (MAY 2006)
Research Article View: 883 Download: 209
Preparation of Nanosilica Powder from Rice Husk Ash by Precipitation Method
page: 206 - 211

Nittaya Thuadaij and Apinon Nuntiya

Vol.35 No.1 (JANUARY 2008)
Research Article View: 2,019 Download: 447
Catalytic Study of Iron, Aluminum, Vanadium and Cobalt Modified Titanium Silicalites-1 in the Hydroxylation of Benzene and Alkyl Benzene by Hydrogen Peroxide
page: 178 - 187

Pornnapa Kasemsiri, Kriangkrai Shenchunthichai, Patchanee Chammingkwanand Tharathon Mongkhonsi

Vol.35 No.1 (JANUARY 2008)
Research Article View: 900 Download: 354
Catalytic Activity of TS-1 on the Hydroxylation of Benzene and Toluene with Hydrogen Peroxide in a Bubble Reactor
page: 163 - 170

Suchitraporn Sakullimcharoen, Panas Manit and Tharathon Mongkhonsi

Vol.35 No.1 (JANUARY 2008)
Research Article View: 949 Download: 310
Experiments and Statistical Analysis of Supercritical Carbon Dioxide Extraction
page: 109 - 115

Wipawee Yothipitak, Praiya Thana, Motonobu Goto and Artiwan Shotipruk

Vol.35 No.1 (JANUARY 2008)
Research Article View: 938 Download: 317
Development of Fuel Briquettes from Biomass-Lignite Blends
page: 43 - 50

Suparin Chaiklangmuang, Suwit Supa and Prattana Kaewpet

Vol.35 No.1 (JANUARY 2008)
Research Article View: 879 Download: 324
Fabrication and Characterization of High Strength Dental Porcelain Nanocomposite from Thailandís Raw Materials
page: 549 - 553

Attavit Pisitanusorn*[a], Supon Ananta [a], Rattikorn Yimnirun [a] and Sakdipown Thiansem [b]

Vol.32 No.3 (SEPTEMBER 2005)
Research Article View: 911 Download: 254
Lithofacies and Fossils of Carboniferous and Permian Carbonate Rocks from the Chiang Dao Area, Northern Thailand
page: 294 - 310

Sutee Jongautchariyakul and Wutti Uttamo

Vol.35 No.2 (MAY 2008)
Research Article View: 953 Download: 1,047
Pressure-Temperature Estimates of the Metamorphosed Sedimentary Rocks on the Eastern Side of Khao Phai, Immediate West of Ban Choeng Chai, Wang Pong, Phetchabun Province, Thailand
page: 283 - 293

Yuenyong Panjasawatwong, Boontarika Srithai and Udomporn Wipakul

Vol.35 No.2 (MAY 2008)
Research Article View: 898 Download: 257
Preparation of Carbon Nanotubes by Catalytic Decomposition of Alcohol at Low Pressure
page: 427 - 432

Pisanunak Chiwsitthiprapai [a], Sutichai Chaisitsak*[a] and Pavan Siamchai [b]

Vol.32 No.3 (SEPTEMBER 2005)
Research Article View: 869 Download: 262
The Uniformity of Carbon Nanotubes Synthesized by Hot Carbon-filament Enhanced CVD
page: 411 - 416

Sutichai Chaisitsak*[a], Akira Y Yamada amada [b] and Mak Makoto oto K Konagai onagai [b]

Vol.32 No.3 (SEPTEMBER 2005)
Research Article View: 876 Download: 260
Synthesis of Carbon Nanoparticles Using Thermal Co-pyrolysis of Ferrocene and Naphthalene Mixture
page: 379 - 383

Tawatchai Charinpanitkul [a]*, Noriaki Sano [b], P ramote Puengjinda [a] +, P oonlasak Muthak arn [

Vol.32 No.3 (SEPTEMBER 2005)
Research Article View: 1,355 Download: 260
Potential of Nanocomposite Technique for Fabrication of Smart Ceramics
page: 179 - 187

Rewadee Wongmaneerung, Laongnuan Srisombat, Rattikorn Yimnirun, and Supon Ananta

Vol.36 No.2 (MAY 2009)
Short Communication View: 870 Download: 341
Chemical Analysis of Airborne Particulates for Air Pollutants in Chiang Mai and Lamphun Provinces, Thailand
page: 123 - 135

Somporn Chantara, Sunanta Wangkarn, Urai Tengcharoenkul, Walaya Sangchan and Mongkon Rayanakorn

Vol.36 No.2 (MAY 2009)
Short Communication View: 980 Download: 270
Self-Reduction of Gold on Activated Carbon Cloth
page: 99 - 105

Surin Saipanya and Thapanee Sarakonsri

Vol.37 No.1 (JANUARY 2010)
Research Article View: 846 Download: 287
A Microscopical Investigation of the Interface Between Borosilicate Glass and Fe-Ni-Co Alloy Joined by Direct Fusion of Glass to Metal
page: 15 - 19

Torranin Chairuangsri*[a], Manat Jaimasith [a], Worapong Thiemsorn [a] and John T.H. Pearce [b] and John T. H. Pearce [b]

Vol.29 No.1 (APRIL 2002)
Research Article View: 891 Download: 272
Determination of Copper by Slurry-Sampling Electro-thermal Atomic Absorption Spectrometry After Pre-concentration on Activated Carbon
page: 65 - 70

Khuanjit Benyatian

Vol.27 No.2 (DECEMBER 2000)
Opinion View: 941 Download: 237
A Barium-Calcium Silicate Glass for Use as Seals in Planar SOFCs
page: 231 - 242

Prachaya Namwong, Nattapol Laorodphan, Worapong Thiemsorn, Manat Jaimasith, Anucha Wannakon, and Tor

Vol.37 No.2 (MAY 2010)
Research Article View: 989 Download: 298
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