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Removal of p-Nitrophenol from Aqueous Solution Using Synthesized Silica-Magnetite Composite


Paper Type 
 Contributed Paper
Title 
 Removal of p-Nitrophenol from Aqueous Solution Using Synthesized Silica-Magnetite Composite
Author 
 Adekola F.A.*, Orimolade B.O.** and Adebayo G.B.
Email 
 fadekola@unilorin.edu.ng; orimoladeben@yahoo.com
Abstract:
Silica-magnetite composite was synthesized as model adsorbent for the removal of p-nitrophenol (p-NP), a problematic toxicant present in effluents from pharmaceutical and allied industries. The adsorption behavior was studied by batch method. Prepared adsorbent was fully characterized using Fourier Transform Infra-red spectroscopy (FTIR), Scanning Electron Microscopy (SEM), X-Ray Diffraction (XRD) and X-Ray Fluorescence.  The optimum conditions of adsorption were determined by investigating the effect of initial p-NP concentration, contact time, adsorbent dose, pH value of aqueous solution and temperature. Adsorption equilibrium time was found to be 60 min. The optimum initial concentration of p-NP was 70 mg/L while the optimum temperature and pH were 30 °C and 2 respectively. The equilibrium adsorption experimental data were fitted best the Langmuir isotherm. The pseudo-second order kinetic model described the adsorption kinetics more effectively. The thermodynamic studies revealed that the adsorption process is spontaneous and feasible. The experimental results have revealed the potential of synthesized material for the removal of p-nitrophenol from aqueous solution.
Start & End Page 
 1028 - 1039
Received Date 
 2015-10-16
Revised Date 
Accepted Date 
 2016-01-24
Full Text 
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Keyword 
 silica, magnetite, p-nitrophenol, adsorption
Volume 
 Vol.44 No.3 (July 2017)
DOI 
Citation 
 F.a. A., B.o. O. and G.b. A., Removal of p-Nitrophenol from Aqueous Solution Using Synthesized Silica-Magnetite Composite, Chiang Mai J. Sci., 2017; 44(3): 1028-1039.
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