Candle Flame Synthesis and Electrochemical Behavior of Chain-like Carbon Nano-onions on 304 Stainless Steel

Saifon Kruehong, Chaiyaput Kruehong, Prinya Chindaprasirt and Apichart Artnaseaw
* Author for corresponding; e-mail address: chaikr@kku.ac.th
Volume: Vol.42 No.3 (JULY 2015)
Research Article
DOI:
Received: 10 November 2013, Revised: -, Accepted: 2 Febuary 2015, Published: -

Citation: Kruehong S., Kruehong C., Chindaprasirt P. and Artnaseaw A., Candle Flame Synthesis and Electrochemical Behavior of Chain-like Carbon Nano-onions on 304 Stainless Steel, Chiang Mai Journal of Science, 2015; 42(3): 745-751.

Abstract

The feasibility of chain-like carbon nano-onions on 304 stainless steel substrate by candle flame synthesis was described. The carbon nanomaterials were synthesized at 600^oC for 180 seconds on the 1 cm × 0.5 cm 304 stainless steel wafers. SEM and TEM analysis results of carbon nanomaterials showed that it was chain-like carbon nano-onions of 40-70 nm in diameter with graphite structure. The ratio of the G and D band intensity (I_G/ I_D) of Raman analysis was 1.03. In addition, the chain-like carbon nano-onions-coated 304 stainless steel was applied as working electrode in three-electrode system. The electrochemical behavior of chain-like carbon nano-onions was characterized by cathodic polarization in KOH and H₃PO₄solutions. Electrocatalytic behavior of chain-like carbon nano-onions on oxygen reduction and hydrogen evolution reaction was presented in comparison with uncoated stainless steel wafer.

Keywords: combustion, candle flame, carbon nanotubes, polarization, electrolysis

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