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An Expeditious and Green Synthesis of 3,3¢-(Arylmethylene)-bis-(4-hydroxycoumarins) Catalyzed by 5-Sulfosalicylic Acid


Paper Type 
 Contributed Paper
Title 
 An Expeditious and Green Synthesis of 3,3¢-(Arylmethylene)-bis-(4-hydroxycoumarins) Catalyzed by 5-Sulfosalicylic Acid
Author 
 Hamzeh Kiyani* and Hassan Darbandi
Email 
 hkiyani@du.ac.ir
Abstract:
The expeditious synthesis of 3,3¢-(arylmethylene)-bis-(4-hydroxycoumarins) via a three-component domino Knoevenagel-Michael reaction (3CDKMR) of various aldehydes and 4-hydroxycoumarin, catalyzed by 5-sulfosalicylic acid (SA) is explored. The reactions were conducted at 80 °C using water as a green and environmentally benign medium. The method has several advantages such as reusability of reaction medium, the avoidance of hazardous organic solvents, readily available reagents, cost-effectiveness, and good to high yields.
Start & End Page 
 1002 - 1010
Received Date 
 2015-06-12
Revised Date 
Accepted Date 
 2015-09-04
Full Text 
   Download
Keyword 
 3,3¢-(arylmethylene)-bis-(4-hydroxycoumarins), 4-hydroxycoumarin, 5-sulfosalicylic acid, three-component reaction, water
Volume 
 Vol.44 No.3 (July 2017)
DOI 
Citation 
 Kiyani H. and Darbandi H., An Expeditious and Green Synthesis of 3,3¢-(Arylmethylene)-bis-(4-hydroxycoumarins) Catalyzed by 5-Sulfosalicylic Acid , Chiang Mai J. Sci., 2017; 44(3): 1002-1010.
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Faculty of Science, Chiang Mai University
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Tel: +6653-943-467




Faculty of Science,
Chiang Mai University




EMAIL
cmjs@cmu.ac.th




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