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Synthesis, Characterization and Antioxidant Activity of 2-Halobenzoyl Thiourea bearing α- and β-Alanine


Paper Type 
 Contributed Paper
Title 
 Synthesis, Characterization and Antioxidant Activity of 2-Halobenzoyl Thiourea bearing α- and β-Alanine
Author 
 Nurziana Ngah*, Nor Azanita Mohamed, and Deny Susanti Darnis
Email 
 nurziana@iium.edu.my
Abstract:
 Six new 2-halobenzoylthiourea compounds bearing α- and β-alanine have been successfully synthesized and characterized using CHNS microelemental analysis and spectroscopic methods including FTIR, UV-Vis and NMR. Microelemental analysis data of the compounds were in agreement with the theoretical values. The FTIR spectra showed the presence of important bands of the compounds while the 1H-NMR and 13C-NMR exhibited the expected chemical shifts. The compounds exerted weak antioxidant activity in DPPH scavenging test and moderate to good activity in β-carotene bleaching test. The inclusion of halogen atoms has facilitated the released of hydrogen atoms and introduction of α- and β-alanine have increased the β-carotene bleaching and DPPH scavenging activities of the compounds.

Start & End Page 
 578 - 584
Received Date 
 2014-07-14
Revised Date 
Accepted Date 
 2014-10-13
Full Text 
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Keyword 
 2-halobenzoyl thiourea, alanine, antioxidant
Volume 
 Vol.43 No.3 (APRIL 2016)
DOI 
Citation 
 Ngah N., Mohamed N.A. and Darnis D.S., Synthesis, Characterization and Antioxidant Activity of 2-Halobenzoyl Thiourea bearing α- and β-Alanine, Chiang Mai J. Sci., 2016; 43(3): 578-584.
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Vol.40 No.3 (JULY 2013) View: 569 Download:197
Development of Sequential Injection Analysis Using Peristaltic Pump and Electrochemical Detection for Antioxidant Capacity Test by ABTS Assay
page: 224 - 231
Author:Jakkrapun Kongkedsuk [a], Apisake Hongwitayakorn [a], Wannarekha Bootnapang [b], Nisachon Boonto [b
Vol.40 No.2 (APRIL 2013) View: 550 Download:213
Antimicrobial and Antioxidant Activities of Methanol, Dichloromethane and Ethyl Acetate Extracts of Scutellaria lindbergii Rech.f.
page: 49 - 59
Author:Bibi Sedigheh Fazly-Bazzaz *[a], Atefeh Arab [b], Seyed Ahmad Emami [c], Javad Asili [c], Mohamad Ha
Vol.40 No.1 (JANUARY 2013) View: 597 Download:245
Antioxidant Potential of Pleurotus porrigens Extract and Application in Sunflower Oil during Accelerated Storage
page: 34 - 48
Author:Hip Seng Yim*[a, b], Fook Yee Chye [b], Mei Lian Liow [a], and Chun Wai Ho [a]
Vol.40 No.1 (JANUARY 2013) View: 614 Download:206
Antioxidant and Sensory Properties of Thai Herbal Teas with emphasis on Thunbergia laurifolia Lindl.
page: 599 - 609
Author:Eric W.C. Chan*, Suit Ying Eng, Yuen Ping Tan, Zhiew Cheng Wong, Phui Yan Lye, and Lea Ngar Tan
Vol.39 No.4 (OCTOBER 2012) View: 644 Download:232
Nutritional and Physicochemical Qualities of Thua Nao (Thai Traditional Fermented Soybean)
page: 562 - 574
Author:Katekan Dajanta1,2, Ekachai Chukeatirote3,* and Arunee Apichartsrangkoon2
Vol.39 No.4 (OCTOBER 2012) View: 556 Download:241
Antioxidant, Antibacterial, Anticancer Activities and Chemical Constituents of the Essential Oil from Mesua ferrea Leaves
page: 455 - 463
Author:Sukanya Keawsa-ard* [a] and Samart Kongtaweelert [b]
Vol.39 No.3 (JULY 2012) View: 656 Download:513
In vitro INHIBITION OF LIPID PEROXIDATION AND THE ANTIOXIDANT SYSTEM OF ENDOPHYTIC FUNGI FROM THAI MEDICINAL PLANTS
page: 429 - 444
Author:Teerayut Theantana [a,b], Duangta Kanjanapothi [c], Saisamorn Lumyong* [b]
Vol.39 No.3 (JULY 2012) View: 608 Download:171
Comparative Analysis of Aqueous Extracts of Amaranth and Coriander in Scavenging Free Radical Activity and Protection of DNA against Oxidative Damage
page: 560 - 571
Author:Asmita Dutta and Mukesh Singh
Vol.38 No.4 (OCTOBER 2011) View: 604 Download:259
Antioxidant Capacity of Broccoli Seeds Grown in Thailand
page: 117 - 122
Author:Sarunya Chuanphongpanich* [a], Maitree Suttajit [b], Sukon Phanichphant [c Duang Buddhasukh [c]
Vol.33 No.1 (JANUARY 2006) View: 605 Download:178
Extraction of Phenolic Compounds from Fruits of Bitter Melon (Momordica charantia ) with Subcritical Water Extraction and Antioxidant Activities of These Extracts
page: 123 - 130
Author:Parichat Budrat and Artiwan Shotipruk
Vol.35 No.1 (JANUARY 2008) View: 585 Download:365
Red Yeast Rice Prepared from Thai Glutinous Rice and the Antioxidant Activities
page: 42 - 49
Author:Em-on Chairote, Griangsak Chairote, and Saisamorn Lumyong
Vol.36 No.1 (JANUARY 2009) View: 655 Download:217
Screening of Antioxidants from Some Thai Vegetables and Herbs
page: 1 - 5
Author:Anchana Chanwitheesuk, Nuansri Rakariyatham*, Aphiwat Teerawutgulrag and Teerapol Wongchanapiboon
Vol.29 No.1 (APRIL 2002) View: 691 Download:229
Antioxidant and Anti-inflammatory Activities of Brown Marine Alga, Padina minor Yamada
page: 507 - 516
Author:Yuwadee Peerapornpisal, Doungporn Amornlerdpison, Utan Jamjai, Tawat Taesotikul, Yanee Pongpaibul,
Vol.37 No.3 (SEPTEMBER 2010) View: 624 Download:263
In vitro Antioxidant Activity of Vitex negundo L. Leaf Extracts
page: 489 - 497
Author:Raghavendra H. Lakshmanashetty, Vijayananda B. Nagaraj, Madhumathi G. Hiremath and Vadlapudi Kumar
Vol.37 No.3 (SEPTEMBER 2010) View: 656 Download:390



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