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Quantitative Phase Analysis and Crystal Structure of DyBCO Ceramics Prepared at Diferent Sintering Conditions


Paper Type 
Contributed Paper
Title 
Quantitative Phase Analysis and Crystal Structure of DyBCO Ceramics Prepared at Diferent Sintering Conditions
Author 
Paitoon Boonsong, Pimpilai Wannasut, Ampika Rachakorn and Anucha Watcharapasorn
Email 
anucha@stanfordalumni.org
Abstract:
 

The DyBCO ceramics were fabricated by solid-state reaction method under a normal air atmosphere using a stoichiometric amount (i.e. Dy:Ba:Cu = 1:2:3) of high-purity Dy2O3, BaCO3 and CuO starting powders, which were previously mixed and calcined at 900oC for 4 h. The green DyBCO pellets were sintered at various sintering temperatures (i.e. 850, 900, 930, 950 and 980oC) for 2 h. The influence of sintering process on phase formation of ceramics was observed by X-ray diffraction (XRD). The quantitative phase analysis of ceramics was analyzed by fitting the XRD pattern using the PowderCell program. The results showed that the DyBa2Cu3O7-δ composition was identified as the main crystalline phase. At higher temperatures (> 950oC), the Dy2BaCuO5 (Dy-211) secondary phase was observed. The relative fraction of various phases was discussed in relation to phase formation and density change. The SEM-EDS/WDS images of ceramics exhibited irregular shaped grains. The average grain size increased from ~2.3 to ~7.0 µm when the sintering temperature was increased. The possibility of stoichiometric change in DyBCO ceramic due to different processing conditions was also discussed in details.

Start & End Page 
1835 - 1842
Received Date 
2017-02-22
Revised Date 
Accepted Date 
2017-04-18
Full Text 
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Keyword 
DyBa2Cu3O7-δ, sintering, ceramic, quantitative phase analysis, crystal structure
Volume 
Vol.45 No.4 (July 2018)
DOI 
Citation 
Boonsong P., Wannasut P., Rachakorn A. and Watcharapasorn A., Quantitative Phase Analysis and Crystal Structure of DyBCO Ceramics Prepared at Diferent Sintering Conditions, Chiang Mai Journal of Science, 2018; 45(4): 1835-1842.
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