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Quantitative Phase Analysis and Crystal Structure of DyBCO Ceramics Prepared at Diferent Sintering Conditions
Paper Type  |
Contributed Paper |
Title |
Quantitative Phase Analysis and Crystal Structure of DyBCO Ceramics Prepared at Diferent Sintering Conditions |
Author |
Paitoon Boonsong, Pimpilai Wannasut, Ampika Rachakorn and Anucha Watcharapasorn |
Email |
anucha@stanfordalumni.org |
|
Abstract: The DyBCO ceramics were fabricated by solid-state reaction method under a normal air atmosphere using a stoichiometric amount (i.e. Dy:Ba:Cu = 1:2:3) of high-purity Dy2O3, BaCO3 and CuO starting powders, which were previously mixed and calcined at 900oC for 4 h. The green DyBCO pellets were sintered at various sintering temperatures (i.e. 850, 900, 930, 950 and 980oC) for 2 h. The influence of sintering process on phase formation of ceramics was observed by X-ray diffraction (XRD). The quantitative phase analysis of ceramics was analyzed by fitting the XRD pattern using the PowderCell program. The results showed that the DyBa2Cu3O7-δ composition was identified as the main crystalline phase. At higher temperatures (> 950oC), the Dy2BaCuO5 (Dy-211) secondary phase was observed. The relative fraction of various phases was discussed in relation to phase formation and density change. The SEM-EDS/WDS images of ceramics exhibited irregular shaped grains. The average grain size increased from ~2.3 to ~7.0 µm when the sintering temperature was increased. The possibility of stoichiometric change in DyBCO ceramic due to different processing conditions was also discussed in details. |
|
Start & End Page |
1835 - 1842 |
Received Date |
2017-02-22 |
Revised Date |
|
Accepted Date |
2017-04-18 |
Full Text |
Download |
Keyword |
DyBa2Cu3O7-δ, sintering, ceramic, quantitative phase analysis, crystal structure |
Volume |
Vol.45 No.4 (July 2018) |
DOI |
|
Citation |
Boonsong P., Wannasut P., Rachakorn A. and Watcharapasorn A., Quantitative Phase Analysis and Crystal Structure of DyBCO Ceramics Prepared at Diferent Sintering Conditions, Chiang Mai Journal of Science, 2018; 45(4): 1835-1842. |
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