Submit your paper 
Download Template JOURNAL DETAIL
Nanocrystalline Hydroxyapatite Powders by a Polymerized Complex Method
Paper Type  |
Contributed Paper |
Title |
Nanocrystalline Hydroxyapatite Powders by a Polymerized Complex Method |
Author |
Jutharatana Klinkaewnarong, and Santi Maensiri |
Email |
santimaensiri@gmail.com |
|
Abstract: Nanocrystalline hydroxyapatite (HAp) powders were successfully synthesized by a polymerized complex method and calcination at 750, 800, 900 and 1,000oC for 12 h. The specific surface areas of the calcined powders obtained by BET adsorption technique were 1.83 - 42.82 m2/g, depending on the calcination temperature and soaking time. The phase composition of the calcined powders was studied by X – ray diffraction (XRD) technique. The XRD results confirmed the formation of HAp phase with a small trace of β–TCP phase. With increasing calcination temperature, the crystallity of the HAp increased, showing the hexagonal structure of HAp with the lattice parameter a in a range of 0.9351 – 0.9446 nm and c of 0.6843 - 0.6906 nm The particle sizes of the powder were found to be 16 – 125 nm and as evaluated by the XRD line broadening technique and were 44 – 1,044 nm as obtained from the BET surface area data. The chemical compositions of the calcined powders were characterized by Raman and FTIR spectroscopies. The Raman spectra showed the phosphate vibration mode (ν1(PO4)) at 963 cm-1 for all the calcined powders. The peaks of the phosphate carbonate and hydroxyl vibration modes were observed in the FTIR spectra for all the calcined powders. The morphology of the powders was spherical of size less than 200 nm, as revealed by TEM. Increasing the calcination temperature resulted in the transition from polycrystalline to single crystalline phase of the HAp, as clearly confirmed by the analysis of TEM diffraction patterns.
|
|
Start & End Page |
243 - 251 |
Received Date |
2009-12-15 |
Revised Date |
|
Accepted Date |
2010-01-19 |
Full Text |
Download |
Keyword |
hydroxyapatite, nanocrystalline powders, bioceramics, polymerized complex method, characterization |
Volume |
Vol.37 No.2 (MAY 2010) |
DOI |
|
Citation |
Klinkaewnarong J., and Maensiri S., Nanocrystalline Hydroxyapatite Powders by a Polymerized Complex Method, Chiang Mai Journal of Science, 2010; 37(2): 243-251. |
SDGs |
|
| View:665 Download:212 | |
RELATED ARTICLE
Phase formations, Compressive Strength and Microstructure of Environmentally Friendly Thai Lopburi Calcined Clay-Limestone Cement Mixes
Article ID: e2024089
Author:Arnon Chaipanich, Nalintip Sansuthum, Phakin Chomyen, Kornnika Wianglor and Supakporn Aodkeng
Vol.51 No.6 (November 2024) View: 953 Download:200
Article ID: e2024089
Author:Arnon Chaipanich, Nalintip Sansuthum, Phakin Chomyen, Kornnika Wianglor and Supakporn Aodkeng
Vol.51 No.6 (November 2024) View: 953 Download:200
SDGs:
Isolation and Preliminary Characterization of Probiotic Isolates from Healthy Thai Adult Feces
Article ID: e2024068
Author:Naruemon Tunsakul, Krit Pongpirul, Lampet Wongsaroj, Chitrasak Kullapanich, Sarn Settachaimongkon and Naraporn Somboonna
Vol.51 No.5 (September 2024) View: 1,233 Download:530
Article ID: e2024068
Author:Naruemon Tunsakul, Krit Pongpirul, Lampet Wongsaroj, Chitrasak Kullapanich, Sarn Settachaimongkon and Naraporn Somboonna
Vol.51 No.5 (September 2024) View: 1,233 Download:530
Increased Antibacterial Activity of Zinc-Silver Doped Hydroxyapatite Synthesized via Ultrasonic in Combination with Sol-Gel Technique using Glutinous Rice as a Template
Article ID: e2024044
Author:Piaw Phatai, Sirilak Kamonwannasit, Sakuntala Siri-udom, Cybelle Morales Futalan, Pongtanawat Khemthong, Saran Youngjan, Teera Butburee, Khongvit Prasitnok and Orrasa Prasitnok
Vol.51 No.3 (May 2024) View: 614 Download:386
Article ID: e2024044
Author:Piaw Phatai, Sirilak Kamonwannasit, Sakuntala Siri-udom, Cybelle Morales Futalan, Pongtanawat Khemthong, Saran Youngjan, Teera Butburee, Khongvit Prasitnok and Orrasa Prasitnok
Vol.51 No.3 (May 2024) View: 614 Download:386
Application of Hydroxyapatite Nanoparticles as Fertilizer Improved Yield Quality of Rice (Oryza sativa L.)
Article ID: e2023053
Author:Sirinapa Pongpeera and Duangkamol Maensiri
Vol.50 No.5 (September 2023) View: 557 Download:452
Article ID: e2023053
Author:Sirinapa Pongpeera and Duangkamol Maensiri
Vol.50 No.5 (September 2023) View: 557 Download:452
Synthesis, Characterization and In Silico Biological and Anticancer Activity of 3-(2-Fluorophenyl)-N-(4-Fluorophenyl)- 7H-[1,2,4] Triazolo[3,4-b] [1,3,4] Thiadiazin-6-Amine
page: 377 - 386
Author:Fahad Hassan Shah, Balasaheb Daniyal Vanjare and Song Ja Kim
Vol.49 No.2 (March 2022) View: 954 Download:479
page: 377 - 386
Author:Fahad Hassan Shah, Balasaheb Daniyal Vanjare and Song Ja Kim
Vol.49 No.2 (March 2022) View: 954 Download:479
Development of Polycaprolactone Infiltrated Anti-Tuberculosis Drug-Loaded 3D-Printed Hydroxyapatite for Localized and Sustained Drug Release in Bone and Joint Tuberculosis Treatment
page: 105 - 121
Author:Faungchat Thammarakcharoen, Autcharaporn Srion, Watchara Chokevivat, Ruedee Hemstapat, Noppawan Phumala Morales and Jintamai Suwanprateeb
Vol.49 No.1 (Special Issue I : Jan 2022) View: 1,283 Download:343
page: 105 - 121
Author:Faungchat Thammarakcharoen, Autcharaporn Srion, Watchara Chokevivat, Ruedee Hemstapat, Noppawan Phumala Morales and Jintamai Suwanprateeb
Vol.49 No.1 (Special Issue I : Jan 2022) View: 1,283 Download:343
A Novel Rapid Ultrasonic Treatment for Acid Protease Extraction from Threadfin Bream and Lizardfish Stomachs and Their Biochemical Characterization
page: 1322 - 1337
Author:Sakonwat Kuepethkaew, Srinivasan Damodaran and Sappasith Klomklao
Vol.48 No.5 (September 2021) View: 1,197 Download:235
page: 1322 - 1337
Author:Sakonwat Kuepethkaew, Srinivasan Damodaran and Sappasith Klomklao
Vol.48 No.5 (September 2021) View: 1,197 Download:235
Fatigue Analysis Model for Applying Bioglass–Hydroxyapatite Biocomposite LCP Bone Fixation Plates to Fix Humeral Shaft Fractures
page: 231 - 251
Author:Siwasit Pitjamit and Wasawat Nakkiew*
Vol.48 No.1 (January 2021) View: 727 Download:427
page: 231 - 251
Author:Siwasit Pitjamit and Wasawat Nakkiew*
Vol.48 No.1 (January 2021) View: 727 Download:427
SDGs:
Low Temperature Fabrication of Brushite by PowderBased Three Dimensional Printing Coupled with Phase
Transformation Process
page: 738 - 751
Author:Autcharaporn Srion, Phee Palanuruksa, Faungchat Thammarakcharoen and Jintamai Suwanprateeb*
Vol.47 No.4 (Special Issue II : July 2020) View: 787 Download:365
page: 738 - 751
Author:Autcharaporn Srion, Phee Palanuruksa, Faungchat Thammarakcharoen and Jintamai Suwanprateeb*
Vol.47 No.4 (Special Issue II : July 2020) View: 787 Download:365
BMP-2 Incorporation into 3D Printed Porous Hydroxyapatite by Rapid Biomimetic Co-Precipitation Technique Using Accelerated Calcium Phosphate Solution
page: 723 - 737
Author:Faungchat Thammarakcharoen and Jintamai Suwanprateeb*
Vol.47 No.4 (Special Issue II : July 2020) View: 776 Download:407
page: 723 - 737
Author:Faungchat Thammarakcharoen and Jintamai Suwanprateeb*
Vol.47 No.4 (Special Issue II : July 2020) View: 776 Download:407
Extraction and Characterization of Natural Cellulosic Fiber From Jipijapa (Carludovica palmata)
page: 579 - 591
Author:Víctor M. Moo-Huchin, Emilio Pérez-Pacheco, Carlos R. Ríos-Soberanis, Luis A. Bello-Pérez, José M. Cervantes-Uc, Mario A. A. Dzul-Cervantes and Raciel J. Estrada-León
Vol.46 No.3 (May 2019) View: 885 Download:312
page: 579 - 591
Author:Víctor M. Moo-Huchin, Emilio Pérez-Pacheco, Carlos R. Ríos-Soberanis, Luis A. Bello-Pérez, José M. Cervantes-Uc, Mario A. A. Dzul-Cervantes and Raciel J. Estrada-León
Vol.46 No.3 (May 2019) View: 885 Download:312
Effect of Composition and Sintering Temperature on the Structure and Properties of Porous Bioactive
Glass Scaffolds
page: 568 - 578
Author:Kerim Emre Öksüz*
Vol.46 No.3 (May 2019) View: 680 Download:214
page: 568 - 578
Author:Kerim Emre Öksüz*
Vol.46 No.3 (May 2019) View: 680 Download:214
Preparation Characterization and Application of Novel TiO2 Membrane in Photocatalytic Reactor
page: 361 - 369
Author:Miao Yingchun*, Xu Xiaolin, Liu Kaiquan, Jin Zhitao, Cheng Yuqin and Zhao Xiyan
Vol.46 No.2 (March 2019) View: 609 Download:188
page: 361 - 369
Author:Miao Yingchun*, Xu Xiaolin, Liu Kaiquan, Jin Zhitao, Cheng Yuqin and Zhao Xiyan
Vol.46 No.2 (March 2019) View: 609 Download:188
Optimization, Purification and Characterization of b-xylanase by a Novel Thermotolerant Strain of Microbispora siamensis, DMKUA 245T
page: 2267 - 2282
Author:Antika Boondaeng, Sukhumaporn Krajangsang, Chanaporn Trakunjae, Thanasak Lomthong, Shinji Tokuyama and Vichien Kitpreechavanich
Vol.45 No.6 (September 2018) View: 685 Download:371
page: 2267 - 2282
Author:Antika Boondaeng, Sukhumaporn Krajangsang, Chanaporn Trakunjae, Thanasak Lomthong, Shinji Tokuyama and Vichien Kitpreechavanich
Vol.45 No.6 (September 2018) View: 685 Download:371
Polarization Sensitive Optical Coherence Tomography for Materials Characterization
page: 2232 - 2237
Author:Kunakorn Palawong, Somchai Sonsupap, Santi Maensiri and Panomsak Meemon
Vol.45 No.5 (Special 2018) View: 752 Download:283
page: 2232 - 2237
Author:Kunakorn Palawong, Somchai Sonsupap, Santi Maensiri and Panomsak Meemon
Vol.45 No.5 (Special 2018) View: 752 Download:283
Response Surface Methodology Based Optimized Purification of the Residual Glycerol from Biodiesel Production Process
page: 1570 - 1582
Author:Muhammad Danish*, Muhammad Waseem Mumtaz [a], Mahpara Fakhar [a] and Umer Rashid*
Vol.44 No.4 (October 2017) View: 856 Download:523
page: 1570 - 1582
Author:Muhammad Danish*, Muhammad Waseem Mumtaz [a], Mahpara Fakhar [a] and Umer Rashid*
Vol.44 No.4 (October 2017) View: 856 Download:523
Physicochemical Properties of Magnesium-doped Hydroxyapatite Nanoparticles Prepared by Incipient Wetness Impregnation Method
page: 1091 - 1099
Author:Jutharatana Klinkaewnarong, Sirilak Kamonwannasit, Piaw Phatai*
Vol.44 No.3 (July 2017) View: 738 Download:269
page: 1091 - 1099
Author:Jutharatana Klinkaewnarong, Sirilak Kamonwannasit, Piaw Phatai*
Vol.44 No.3 (July 2017) View: 738 Download:269
Bioactivity, Cytotoxicity and Antibacterial Evaluation of Undoped, Zn-doped, Sr-doped, and
Zn/Sr-codoped Hydroxyapatites Synthesized by a Sol-gel Method
page: 630 - 639
Author:Likit Temprom [a], Suphasinee L. Seet [a,b,c], Patcharaporn Tippayawat [d], Pimsiree Suwanna* [a,b,
Vol.44 No.2 (April 2017) View: 771 Download:205
page: 630 - 639
Author:Likit Temprom [a], Suphasinee L. Seet [a,b,c], Patcharaporn Tippayawat [d], Pimsiree Suwanna* [a,b,
Vol.44 No.2 (April 2017) View: 771 Download:205
Production and Characterization of Bacteriocin-producing Bacteria Capable of Inhibition of Streptococcus dysgalactiae
page: 366 - 374
Author:Nalin Wongkattiya [a], Ian H. Fraser [b], Piyanuch Niamsup [a], Phanchana Sanguansermsri [c] and Don
Vol.44 No.2 (April 2017) View: 709 Download:360
page: 366 - 374
Author:Nalin Wongkattiya [a], Ian H. Fraser [b], Piyanuch Niamsup [a], Phanchana Sanguansermsri [c] and Don
Vol.44 No.2 (April 2017) View: 709 Download:360
Preparation of Nano-hydroxyapatite Particles by Ultrasonic Method at 25 kHz Using Natural Rubber Latex as a Templating Agent
page: 320 - 328
Author:Songkot Utara [a,b]*, Jutharatana Klinkaewnarong [a,c]
Vol.43 No.2 (SPECIAL ISSUE 1) View: 721 Download:236
page: 320 - 328
Author:Songkot Utara [a,b]*, Jutharatana Klinkaewnarong [a,c]
Vol.43 No.2 (SPECIAL ISSUE 1) View: 721 Download:236
Enhancing coating property and storage stability of non-alkoxide sol-gel derived hydroxyapatite coating by incorporating gel retarding agents.
page: 1341 - 1351
Author:Jintamai Suwanprateeb*, Waraporn Suvannapruk, Faungchat Thammarakcharoen and Watchara Chokevivat
Vol.41 No.5/2 (OCTOBER 2014) View: 664 Download:243
page: 1341 - 1351
Author:Jintamai Suwanprateeb*, Waraporn Suvannapruk, Faungchat Thammarakcharoen and Watchara Chokevivat
Vol.41 No.5/2 (OCTOBER 2014) View: 664 Download:243
Purification and Characterization of Fungal Laccase from Mycena purpureofusca
page: 151 - 160
Author:Shujing Sun1, Yonghui Zhang1, Youxiong Que2, Bixian Liu1, Kaihui Hu1, and Liping Xu2*
Vol.40 No.2 (APRIL 2013) View: 703 Download:196
page: 151 - 160
Author:Shujing Sun1, Yonghui Zhang1, Youxiong Que2, Bixian Liu1, Kaihui Hu1, and Liping Xu2*
Vol.40 No.2 (APRIL 2013) View: 703 Download:196
Monodispersity and Stability of Gold Nanoparticles Stabilized by Using Polyvinyl Alcohol
page: 31 - 38
Author:Pichitchai Pimpang, Supab Choopun
Vol.38 No.1 (JANUARY 2011) View: 648 Download:194
page: 31 - 38
Author:Pichitchai Pimpang, Supab Choopun
Vol.38 No.1 (JANUARY 2011) View: 648 Download:194
Preparation and Characterization of HAP-Glass
Porous Composites
page: 495 - 500
Author:Charussri Lorprayoon* and Shigeki Morimoto
Vol.32 No.3 (SEPTEMBER 2005) View: 663 Download:185
page: 495 - 500
Author:Charussri Lorprayoon* and Shigeki Morimoto
Vol.32 No.3 (SEPTEMBER 2005) View: 663 Download:185
Cloning and Expression of Protease Gene from Thermophilic Bacterium Bacillus stearothermophilus TLS33 in Escherichia coli DH5α
page: 53 - 59
Author:Thammarat Kaosombat [a], Supachok Sinchaikul [b], Hataichanoke Niamsup [a], Shui – Tein Chen [b] and Suree Phutrakul* [a]
Vol.29 No.2 (AUGUST 2002) View: 1,109 Download:239
page: 53 - 59
Author:Thammarat Kaosombat [a], Supachok Sinchaikul [b], Hataichanoke Niamsup [a], Shui – Tein Chen [b] and Suree Phutrakul* [a]
Vol.29 No.2 (AUGUST 2002) View: 1,109 Download:239
Copyrights © Since 2021 All Rights Reserved by Chiang Mai Journal of Science