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Synthesis, Characterization, and Crystal Structure Determination of Mercury(II) Complex Containing 2-(Aminomethyl)pyridine
Paper Type  |
Contributed Paper |
Title |
Synthesis, Characterization, and Crystal Structure Determination of Mercury(II) Complex Containing 2-(Aminomethyl)pyridine |
Author |
Sadif A Shirvan, Fereydoon Khazali, Sara Haydari Dezfuli and Ali Borsalani |
Email |
s.shirvan2015@gmail.com |
|
Abstract: The new complex of [Hg(2-AMPy)I2] (1) was synthesized from the reaction of HgI2 with 2-(aminomethyl)pyridine (2-AMPy) in methanolic solution. Suitable crystals of 1 for diffraction experiment were obtained by slow evaporation from DMSO. Resulted complex was characterized by spectral methods (IR and 1H NMR), elemental analysis, thermal analysis and single crystal X-ray diffraction method. In this compound, four coordinated arrangement of the Hg(II) center can be described as a seesaw geometry with the four-coordinate geometry index, t4, of 0.77. |
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Start & End Page |
421 - 426 |
Received Date |
2016-03-25 |
Revised Date |
|
Accepted Date |
2017-02-13 |
Full Text |
Download |
Keyword |
Hg(II), 2-(aminomethyl)pyridine ligand, crystal structure, thermal gravimetric analyses |
Volume |
Vol.45 No.1 (January 2018) |
DOI |
|
Citation |
Shirvan S.A., Khazali F., Dezfuli S.H. and Borsalani A., Synthesis, Characterization, and Crystal Structure Determination of Mercury(II) Complex Containing 2-(Aminomethyl)pyridine, Chiang Mai Journal of Science, 2018; 45(1): 421-426. |
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