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Study the Stable Diatomite-supported Catalyst for Biodiesel Production


Paper Type 
 Contributed Paper
Title 
 Study the Stable Diatomite-supported Catalyst for Biodiesel Production
Author 
 Wilasinee Kingkam, Kewalee Nilgumhang, Sasikarn Nuchdang, Bheechanat Duangdee, Vichai Puripunyavanich and Dussadee Rattanaphra
Email 
 dussadee@tint.or.th
Abstract:

     The stable of natural diatomite supported by potassium hydroxide (KOH) as catalysts were synthesized for biodiesel production. A heterogeneous base catalyst prepared by impregnating KOH onto diatomite was also used to synthesize biodiesel from palm oil. All samples have been thoroughly characterized by Wavelength Dispersive X-ray Fluorescence (WDXRF), X-ray diffraction (XRD), N2 adsorption/desorption, Scanning electron microscopy (SEM), Energy dispersive spectrometer (EDS), and Temperature-programmed desorption of carbon dioxide (CO2-TPD). The XRD, XRF, and SEM results confi rm that adding KOH to diatomite results in structural change. The SiO2 and K2O phases form in the diatomite structural matrix during impregnation and the total basicity amount of this compound promotes the transesterifi cation process. A maximum fatty acid methyl ester (FAME) content of 84.56% was obtained. The reaction conditions were as follows: molar ratio of oil to methanol 1:9, catalyst loading 5 wt%, reaction time 2 h, and reaction temperature 75 °C. This work provides a possible new method for converting KOH from a homogeneous to a heterogeneous catalyst (Diatomite/KOH) that may show stable reusability, avoiding the separation and pollution problems in the environment.
Start & End Page 
 1332 - 1343
Received Date 
 2022-05-11
Revised Date 
 2022-08-17
Accepted Date 
 2022-08-22
Full Text 
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Keyword 
 impregnation, diatomite, transesterification, heterogeneous catalyst, biodiesel
Volume 
 Vol.49 No.5 (September 2022)
DOI 
 https://doi.org/10.12982/CMJS.2022.083
Citation 
 Kingkam W., Nilgumhang K., Nuchdang S., Duangdee B., Puripunyavanich V. and Rattanaphra D., Study the Stable Diatomite-supported Catalyst for Biodiesel Production, Chiang Mai Journal of Science, 2022; 49(5): 1332-1343. DOI 10.12982/CMJS.2022.083.
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