Chiang Mai Journal of Science, Faculty of Science, Chiang Mai University

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Investigation of Metastable Zone Width and Nucleation Kinetics of 2-cyanoguanidine by Cooling Crystallization

Paper Type	Contributed Paper
Title	Investigation of Metastable Zone Width and Nucleation Kinetics of 2-cyanoguanidine by Cooling Crystallization
Author	Ning Zhang, Yongsheng Ren*, Chengqi Liu and Haipeng Zhao
Email	renys@nxu.edu.cn; ys-ren@126.com
Abstract: Metastable zone widths (MSZW) of 2-cyanoguanidine in water, methanol, and ethanol are determined at different cooling rates ((6-30) K×h-1) using polythermal method, respectively. The metastable zone widths of solute in the three solvents increase linearly with the cooling rate increasing. Three nucleation theories are employed to estimate nucleation kinetic parameters based on measured MSZW data. The apparent nucleation order m is computed by Self-consistent Nývlt-like approach and Kubota’s model, which suggests that the nuclei are formed by instantaneous nucleation in methanol and ethanol, while the 2-cyanoguanidine nucleate in water shows the occurrence of progressive nucleation mechanism. The activation energy Esat for nucleation of crystals in solution also is estimated by Arrhenius-type equation.
Start & End Page	1633 - 1645
Received Date	2015-10-22
Revised Date
Accepted Date	2016-02-24
Full Text	Download
Keyword	2-cyanoguanidine, metastable zone width, nucleation kinetics, model
Volume	Vol.44 No.4 (October 2017)
DOI
Citation	Zhang N., Ren* Y., Liu C. and Zhao H., Investigation of Metastable Zone Width and Nucleation Kinetics of 2-cyanoguanidine by Cooling Crystallization , Chiang Mai Journal of Science, 2017; 44(4): 1633-1645.
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Investigation of Metastable Zone Width and Nucleation Kinetics of 2-cyanoguanidine by Cooling Crystallization

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