Submit your paper 
Download Template JOURNAL DETAIL
A Simple Dispersive Micro-Solid Phase Extraction for Determination of Neonicotinoid Insecticides in Surface Water and Fruit Juice Samples
Paper Type  |
Contributed Paper |
Title |
A Simple Dispersive Micro-Solid Phase Extraction for Determination of Neonicotinoid Insecticides in Surface Water and Fruit Juice Samples |
Author |
Jitlada Vichapong, Yanawath Santaladchaiyakit, Rodjana Burakham and Supalax Srijaranai |
Email |
jitlada.v@msu.ac.th |
|
Abstract: A dispersive micro-solid phase extraction (D-μ-SPE) has been investigated for simple microextraction and preconcentration of fi ve neonicotinoid insecticides residues followed by highperformance liquid chromatography. The neonicotinoid insecticides including thiamethoxam, clothianidin, imidacloprid, acetamiprid, and thiacloprid, were separated on LiChroprep® 100 RP-8 endcapped column using 25% (v/v) acetonitrile with a fl ow rate of 1.0 mL min−1. LiChroprep® RP-18 (C-18) was chosen as an effi cient adsorbent in d-μ-SPE. The experimental parameters affecting the extraction performance of D-μ-SPE were investigated including salt addition, amount of sorbent, sample volume, and kind and volume of desorption solvent. Under the selected conditions, linearity was found in the range of 0.003-0.1 μg mL−1. Low limit of detection and high enrichment factor (11 – 81) were obtained. The proposed method was successfully applied for the determination of neonicotinoid insecticide residues in surface water and fruit juice samples with high obtained recoveries. |
|
Start & End Page |
387 - 397 |
Received Date |
2021-05-28 |
Revised Date |
2022-01-05 |
Accepted Date |
2022-01-21 |
Full Text |
Download |
Keyword |
sample preparation, sorbent, HPLC, thiamethoxam, clothianidin, imidacloprid, acetamiprid, thiacloprid |
Volume |
Vol.49 No.2 (March 2022) |
DOI |
https://doi.org/10.12982/CMJS.2022.037 |
Citation |
Vichapong J., Santaladchaiyakit Y., Burakham R. and Srijaranai S., A Simple Dispersive Micro-Solid Phase Extraction for Determination of Neonicotinoid Insecticides in Surface Water and Fruit Juice Samples, Chiang Mai Journal of Science, 2022; 49(2): 387-397. DOI 10.12982/CMJS.2022.037. |
SDGs |
|
| View:1,514 Download:352 | |
RELATED ARTICLE
Degradation of Dimethyl Phthalate and Diethyl Phthalate by Bacteria Isolated from Jazan, Saudi Arabia
Article ID: e2024025
Author:Nouf A. AL Awaji, Mohammed D. Y. Oteef and Ashraf M. M. Essa
Vol.51 No.2 (March 2024) View: 660 Download:390
Article ID: e2024025
Author:Nouf A. AL Awaji, Mohammed D. Y. Oteef and Ashraf M. M. Essa
Vol.51 No.2 (March 2024) View: 660 Download:390
Hydrogen Sulfide Adsorption on Alumina/Graphene Oxide Composites at Ambient Temperature
page: 1618 - 1632
Author:Montree Hankoy, Mettaya Kitiwan, Chaiwat Phrompet, Chesta Ruttanapun, Prangtip Rittichote Kaewpengkrow, Supawan Vichaphund, Duangduen Atong and Phacharaphon Tunthawiroon
Vol.49 No.6 (November 2022) View: 1,873 Download:427
page: 1618 - 1632
Author:Montree Hankoy, Mettaya Kitiwan, Chaiwat Phrompet, Chesta Ruttanapun, Prangtip Rittichote Kaewpengkrow, Supawan Vichaphund, Duangduen Atong and Phacharaphon Tunthawiroon
Vol.49 No.6 (November 2022) View: 1,873 Download:427
Adsorption of 2,4-Dichlorophenoxyacetic acid by Magnesium Ferrite Magnetic Nanoparticles Modified with Amine Functional Groups
page: 137 - 146
Author:Supawitch Hoijang, Jeeranan Nonkumwong, Burapol Singhana, Sunanta Wangkarn, Supon Ananta and Laongnuan Srisombat
Vol.47 No.1 (January 2020) View: 1,315 Download:436
page: 137 - 146
Author:Supawitch Hoijang, Jeeranan Nonkumwong, Burapol Singhana, Sunanta Wangkarn, Supon Ananta and Laongnuan Srisombat
Vol.47 No.1 (January 2020) View: 1,315 Download:436
SDGs:
A Comparison of Three Extraction Methods for Phenolic Compounds and Antioxidant Activities
from Moringa oleifera Leaves
page: 2779 - 2789
Author:Truong Kim Tai, Jittima Thongklay, Pisipong Meunprasertdee, Papadchaya Kornthattalim and Thammarat Kaaewmanee
Vol.45 NO.7 (November 2018) View: 903 Download:848
page: 2779 - 2789
Author:Truong Kim Tai, Jittima Thongklay, Pisipong Meunprasertdee, Papadchaya Kornthattalim and Thammarat Kaaewmanee
Vol.45 NO.7 (November 2018) View: 903 Download:848
HS-SPME for the Determination of Phthalate Esters in Vegetable Oil and Soft Drink Samples
page: 1052 - 1061
Author:Sutthirak Uansiri, Jitlada Vichapong and Wanna Kanchanamayoon*
Vol.45 No.2 (March 2018) View: 778 Download:236
page: 1052 - 1061
Author:Sutthirak Uansiri, Jitlada Vichapong and Wanna Kanchanamayoon*
Vol.45 No.2 (March 2018) View: 778 Download:236
Greener, Rapid and Reliable UHPLC using 1-alkyl-3-methylimidazolium-based Ionic Liquids as the Mobile Phase Additives for Simultaneous Determination of Steroids and Antihistamines Residues in Herbal Medicines
page: 380 - 403
Author:Krittaya Nusai and Prayong Doungdee
Vol.45 No.1 (January 2018) View: 732 Download:277
page: 380 - 403
Author:Krittaya Nusai and Prayong Doungdee
Vol.45 No.1 (January 2018) View: 732 Download:277
Subcritical Water Extraction Technique for Selective Extraction of Pentacyclic Triterpenoids from Dry Loquat (Eriobotrya japonica) Leaves
page: 1534 - 1547
Author:Erasto Mlyuka, Shuang Zhang, Zongping Zheng, Zhiyong He, Maomao Zeng, Martha Mbifile and Jie Chen*
Vol.44 No.4 (October 2017) View: 737 Download:310
page: 1534 - 1547
Author:Erasto Mlyuka, Shuang Zhang, Zongping Zheng, Zhiyong He, Maomao Zeng, Martha Mbifile and Jie Chen*
Vol.44 No.4 (October 2017) View: 737 Download:310
A Simple High-performance Liquid Chromatography Coupled to Fluorescence Detection Method using Column-switching Technique for Measuring Urinary 1-hydroxypyrene from Environmental Exposure
page: 1441 - 1452
Author:Kunrunya Sutan*, Warangakana Naksen* and Tippawan Prapamontol+
Vol.44 No.4 (October 2017) View: 720 Download:286
page: 1441 - 1452
Author:Kunrunya Sutan*, Warangakana Naksen* and Tippawan Prapamontol+
Vol.44 No.4 (October 2017) View: 720 Download:286
Antioxidant Activities and Stability of Seed Kernel Extracts from Mango (Mangifera indica linn.) Cultivated in Northern Thailand
page: 573 - 583
Author:Nichana Nakpanich, Wantida Chaiyana and Pimporn Leelapornpisid*
Vol.44 No.2 (April 2017) View: 767 Download:288
page: 573 - 583
Author:Nichana Nakpanich, Wantida Chaiyana and Pimporn Leelapornpisid*
Vol.44 No.2 (April 2017) View: 767 Download:288
Evaluation of Treated and Untreated Sludge from Yarn Processing Factory as Adsorbent Candidates for Dye Removal
page: 508 - 517
Author:Muhammad Abbas Ahmad Zaini* [a,b] and Noor Yuhana Jusoh [b]
Vol.44 No.2 (April 2017) View: 1,167 Download:198
page: 508 - 517
Author:Muhammad Abbas Ahmad Zaini* [a,b] and Noor Yuhana Jusoh [b]
Vol.44 No.2 (April 2017) View: 1,167 Download:198
Blazeispirol A, a Chemotaxonomic Marker from Mycelia of the Medicinal Mushroom Agaricus subrufescens
page: 298 - 308
Author:Naritsada Thongklang [a,b], Benjarong Thongbai [a,b], Sunita Chamyuang [b], Philippe Callac [c], Eka
Vol.44 No.2 (April 2017) View: 774 Download:244
page: 298 - 308
Author:Naritsada Thongklang [a,b], Benjarong Thongbai [a,b], Sunita Chamyuang [b], Philippe Callac [c], Eka
Vol.44 No.2 (April 2017) View: 774 Download:244
Development and Validation of HPLC with UV Detection Method: Analysis of Cilazparil in Pharmaceutical Dosage Forms
page: 1142 - 1149
Author:Petikam Lavudu [a], Avula Prameela Rani [b], Chandra Bala Sekaran [c]*
Vol.43 No.5 (OCTOBER 2016) View: 758 Download:275
page: 1142 - 1149
Author:Petikam Lavudu [a], Avula Prameela Rani [b], Chandra Bala Sekaran [c]*
Vol.43 No.5 (OCTOBER 2016) View: 758 Download:275
Effect of Temperature on Schizophyllum commune Growth and 4H-pyran-4-one,2,3-dihydro-3, 5-dihydroxy-6-methyl- Production using a Bubble Column Bioreactor
page: 462 - 469
Author:Yi Peng Teoh and Mashitah Mat Don*
Vol.43 No.3 (APRIL 2016) View: 676 Download:309
page: 462 - 469
Author:Yi Peng Teoh and Mashitah Mat Don*
Vol.43 No.3 (APRIL 2016) View: 676 Download:309
Fatty Acid, Essential Oil and Phenolic Compositions of Alcea pallida and Alcea apterocarpa with Antioxidant, Anticholinesterase and Antimicrobial Activities
page: 89 - 99
Author:Abdulselam Ertas*[a,b], Mehmet Boga [b,c], Isil Gazioglu [d], Yeter Yesil [e] , Nesrin Hasimi [f], Cumali Ozaslan [g], Hasibe Yilmaz[h], Muammer Kaplan[j]
Vol.43 No.1 (JANUARY 2016) View: 720 Download:282
page: 89 - 99
Author:Abdulselam Ertas*[a,b], Mehmet Boga [b,c], Isil Gazioglu [d], Yeter Yesil [e] , Nesrin Hasimi [f], Cumali Ozaslan [g], Hasibe Yilmaz[h], Muammer Kaplan[j]
Vol.43 No.1 (JANUARY 2016) View: 720 Download:282
A Sensitive Method for Determination of Carbendazim Residue in Vegetable Samples using HPLC-UV and Its Application in Health Risk Assessment
page: 681 - 690
Author:Buran Phansawan, Tippawan Prapamontol, Prasak Thavonyutikarn, Somporn Chantara,
Vol.42 No.3 (JULY 2015) View: 751 Download:376
page: 681 - 690
Author:Buran Phansawan, Tippawan Prapamontol, Prasak Thavonyutikarn, Somporn Chantara,
Vol.42 No.3 (JULY 2015) View: 751 Download:376
Effect of temperature on Schizophyllum commune growth and 4H-pyran-4-one,2,3-dihydro-3,5-dihydroxy-6-methyl- production using a bubble column bioreactor
page: 539 - 548
Author:Yi Peng, Teoh and Mashitah, Mat Don
Vol.42 No.3 (JULY 2015) View: 667 Download:254
page: 539 - 548
Author:Yi Peng, Teoh and Mashitah, Mat Don
Vol.42 No.3 (JULY 2015) View: 667 Download:254
Removal of Methylene Blue from Aqueous Solution by Coffee Residues
page: 407 - 416
Author:Walaikorn Nitayaphat, Thanut Jintakosol, Kamontip Engkaseth and Yada Wanrakakit
Vol.42 No.2 (APRIL 2015) View: 824 Download:271
page: 407 - 416
Author:Walaikorn Nitayaphat, Thanut Jintakosol, Kamontip Engkaseth and Yada Wanrakakit
Vol.42 No.2 (APRIL 2015) View: 824 Download:271
Phenolic Compounds, Biological and Antioxidant Activities of Onobrychis armena Boiss. & Huet Flower and Root Extracts
page: 376 - 392
Author:Kubra Karakoca, Meltem Asan-Ozusaglam, Yavuz Selim Cakmak and Mehtap Teksen
Vol.42 No.2 (APRIL 2015) View: 670 Download:235
page: 376 - 392
Author:Kubra Karakoca, Meltem Asan-Ozusaglam, Yavuz Selim Cakmak and Mehtap Teksen
Vol.42 No.2 (APRIL 2015) View: 670 Download:235
Determination of Organic Acids in Avocado Fermented Juice by High Performance Liquid Chromatography
page: 208 - 215
Author:Pichai Liawruangrath, Boonsom Liawruangrath and Saisunee Liawruangrath
Vol.42 No.1 (JANUARY 2015) View: 671 Download:265
page: 208 - 215
Author:Pichai Liawruangrath, Boonsom Liawruangrath and Saisunee Liawruangrath
Vol.42 No.1 (JANUARY 2015) View: 671 Download:265
Enhanced Production of Polysaccharides and Protein Content in Cyanobacterium, Oscillatoria limnetica as a Defense Mechanism Against Low pH and Pb2+
page: 34 - 43
Author:Suneerat Ruangsomboon*
Vol.42 No.1 (JANUARY 2015) View: 1,096 Download:202
page: 34 - 43
Author:Suneerat Ruangsomboon*
Vol.42 No.1 (JANUARY 2015) View: 1,096 Download:202
Antioxidative Properties and HPLC Profile of Chloroform Fraction from Ethanolic Extract of the Peel of Citrus hystrix
page: 173 - 184
Author:Kah Weng Chua [a], Chiaw Mei Sia [a], Gabriel A. Akowuah [b], Loshnie Samuagam [a], and Hip Seng Yim
Vol.42 No.1 (JANUARY 2015) View: 720 Download:320
page: 173 - 184
Author:Kah Weng Chua [a], Chiaw Mei Sia [a], Gabriel A. Akowuah [b], Loshnie Samuagam [a], and Hip Seng Yim
Vol.42 No.1 (JANUARY 2015) View: 720 Download:320
Zearalenone Contamination in Corn for Human Consumption in Kamphaengphet, Thailand
page: 534 - 539
Author:Wachira Singkong*[a], Hastin Ratanapol [a] and Wachira Liamkaew [b]
Vol.40 No.3 (JULY 2013) View: 687 Download:185
page: 534 - 539
Author:Wachira Singkong*[a], Hastin Ratanapol [a] and Wachira Liamkaew [b]
Vol.40 No.3 (JULY 2013) View: 687 Download:185
Optimization Method for Determination of Carbofuran
and Carboxin Residues in Cabbages by SPE and
HPLC-UV
page: 227 - 234
Author:Khin L. Zan, and Somporn Chantara
Vol.34 No.2 (MAY 2007) View: 671 Download:230
page: 227 - 234
Author:Khin L. Zan, and Somporn Chantara
Vol.34 No.2 (MAY 2007) View: 671 Download:230
High Performance Liquid Chromatographic Analysis
of Asiaticoside in Centella asiatica (L.) Urban
page: 521 - 525
Author:Prateek K. Jain and Ram K. Agrawal
Vol.35 No.3 (SEPTEMBER 2008) View: 707 Download:416
page: 521 - 525
Author:Prateek K. Jain and Ram K. Agrawal
Vol.35 No.3 (SEPTEMBER 2008) View: 707 Download:416
Partitioning Behaviour of Chlorinated Hydrocarbon in
HPLC as Related to Soil/Water Partitioning
page: 61 - 70
Author:Maliwan Boonsaner
Vol.32 No.1 (JANUARY 2005) View: 648 Download:199
page: 61 - 70
Author:Maliwan Boonsaner
Vol.32 No.1 (JANUARY 2005) View: 648 Download:199
Solid Phase Extraction of Carbamate and Organochlorine Pesticides in Water
page: 9 - 15
Author:Wanna Kanchanamayoon, Sirichai Hathongkam and Amnat Laothong
Vol.28 No.1 (JUNE 2001) View: 666 Download:289
page: 9 - 15
Author:Wanna Kanchanamayoon, Sirichai Hathongkam and Amnat Laothong
Vol.28 No.1 (JUNE 2001) View: 666 Download:289
Retention Behavior of Aromatic Amines with Some Ionic Liquids Mobile Phase in Semi-micro HPLC
page: 384 - 396
Author:Yuppadee Nusai, Hitoshi Koizumi, Masaki Tachibana, Kazue Tani, and Nobutoshi Kiba
Vol.37 No.3 (SEPTEMBER 2010) View: 729 Download:221
page: 384 - 396
Author:Yuppadee Nusai, Hitoshi Koizumi, Masaki Tachibana, Kazue Tani, and Nobutoshi Kiba
Vol.37 No.3 (SEPTEMBER 2010) View: 729 Download:221
Copyrights © Since 2021 All Rights Reserved by Chiang Mai Journal of Science