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Effect of Sintering Conditions on Densification and Dielectric Properties of PZT Ceramics


Paper Type 
Contributed Paper
Title 
Effect of Sintering Conditions on Densification and Dielectric Properties of PZT Ceramics
Author 
Rungnapa Tipakontitikul*, Supon Ananta and Rattikorn Yimnirun
Email 
rungnapa@rocketmail.com
Abstract:
Complex perovskite-like phase of lead zirconate titanate, Pb(Zr,Ti)O3  (PZT) ceramics were fabricated with a mixed oxide synthetic route of zirconium titanate (ZrTiO4 ) and lead oxide (PbO) precursors. The effects of sintering conditions on phase formation, densification and dielectric response of PZT ceramics have been investigated using XRD, SEM, EDX and dielectric measurement techniques. The experimental results show that the densification of the PZT ceramics with density 97 % theoretical density, without any sintering additives, can be achieved with appropriate sintering condition (the optimum sintering condition has been identified as 1,225°C for 4 h). The dielectric properties increases with increasing sintering temperature and grain size. However, over 1250 °C, dielectric properties decreased due to PbO vaporization.
Start & End Page 
323 - 329
Received Date 
Revised Date 
Accepted Date 
Full Text 
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Keyword 
lead zirconate titanate, perovskite, PZT
Volume 
Vol.32 No.3 (SEPTEMBER 2005)
DOI 
Citation 
Tipakontitikul* R.., Ananta S.. and Yimnirun R.., Effect of Sintering Conditions on Densification and Dielectric Properties of PZT Ceramics, Chiang Mai Journal of Science, 2005; 32(3): 323-329.
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