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Characterization of Perovskite Lead Iron Niobate Powders Synthesized by Partial Oxalate
Paper Type  |
Short Communication |
Title |
Characterization of Perovskite Lead Iron Niobate Powders Synthesized by Partial Oxalate |
Author |
Pitak Youmee [a] and Sukon Phanichphant* [b] |
Email |
psukon@yahoo.com |
|
Abstract: A partial oxalate route has been developed for the synthesis of lead iron niobate, Pb(Fe1/2Nb1/2)O3 (PFN) powder. An oxalated iron niobate (FeNbO4) was employed as a key precursor with the formation of PFN phase investigated as a function of calcination temperature and dwell time by TG-DTA and XRD. The morphology of the calcined powder was determined via SEM. It has been found that the unreacted FeNbO4 and PbO phases tend to form together with PFN depending on calcination conditions. However, single phase PFN powder was successfully obtained for a calcination temperature of 900°C for 4 h.
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|
Start & End Page |
71 - 76 |
Received Date |
2004-08-30 |
Revised Date |
|
Accepted Date |
2005-01-04 |
Full Text |
Download |
Keyword |
lead iron niobate, perovskite, PFN, phase formation, powder chemical-synthetic |
Volume |
Vol.32 No.1 (JANUARY 2005) |
DOI |
|
Citation |
Youmee P. and Phanichphant S., Characterization of Perovskite Lead Iron Niobate Powders Synthesized by Partial Oxalate, Chiang Mai J. Sci., 2005; 32(1): 71-76. |
SDGs |
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| View:571 Download:161 | |
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