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Phase and Chemical Characterization of Perovskite Lead Nickel Niobate Ceramics Fabricated Via a Columbite Precursor Method


Paper Type 
Contributed Paper
Title 
Phase and Chemical Characterization of Perovskite Lead Nickel Niobate Ceramics Fabricated Via a Columbite Precursor Method
Author 
Laongnuan Srisombat, Orawan Khamman, Rattikorn Yimnirun, Supon Ananta, and T. Randall Lee Rungsun Nu
Email 
slaongnuan@yahoo.com
Abstract:
Perovskite relaxor ferroelectric lead nickel niobate (PNN) ceramics were fabricated by using B-site precursor method, in which columbite-NiNb2O6 was employed as key precursor. It has been found that optimization of sintering condition can successfully lead to highly dense PNN ceramics. Although XRD analysis revealed that the ceramics consist of  pure perovskite phase, significant fluctuation in chemical composition, precipitation of  unreacted precursor and the formation of  unwanted phases were found via a combination between SEM EDX and XPS techniques
Start & End Page 
69 - 76
Received Date 
2008-11-01
Revised Date 
Accepted Date 
2008-12-15
Full Text 
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Keyword 
lead nickel niobate, perovskite, columbite precursor, chemical characteristic
Volume 
Vol.36 No.1 (JANUARY 2009)
DOI 
Citation 
Srisombat L., Khamman O., Yimnirun R., Ananta S., and Nu T.R.L.R., Phase and Chemical Characterization of Perovskite Lead Nickel Niobate Ceramics Fabricated Via a Columbite Precursor Method, Chiang Mai Journal of Science, 2009; 36(1): 69-76.
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