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Hydrothermal Synthesis of Lead Titanate Fine Powders at Water Boiling Temperature


Paper Type 
Contributed Paper
Title 
Hydrothermal Synthesis of Lead Titanate Fine Powders at Water Boiling Temperature
Author 
Chaiyos Chankaew, and Apinpus Rujiwatra
Email 
apinpus@gmail.com
Abstract:
Lead titanate fine powders comprising of a single tetragonal phase and well characterized particles were successfully synthesized at an exceptionally low temperature of 100oC. The important role of  the ultrasonication in reducing the thermodynamic barrier of the hydrothermal reaction, and the slow rate of  hydrothermal reaction at 100oC were underlined. The synthesized particles were revealed to be tetragonal in shape, mostly submicrometers in size, and generally present as large aggregates. The layer-by-layer model was also proposed as the particle growth mechanism.
Start & End Page 
92 - 98
Received Date 
2009-06-10
Revised Date 
Accepted Date 
2009-07-22
Full Text 
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Keyword 
lead titanate, perovskite, ultrasonication, hydrothermal synthesis
Volume 
Vol.37 No.1 (JANUARY 2010)
DOI 
Citation 
Chankaew C. and Rujiwatra A., Hydrothermal Synthesis of Lead Titanate Fine Powders at Water Boiling Temperature, Chiang Mai J. Sci., 2010; 37(1): 92-98.
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Chiang Mai Journal of Science

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