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Characterization of Nitrate Route Synthesized Lead Zirconate Titanate Powders and Ceramics


Paper Type 
Opinion
Title 
Characterization of Nitrate Route Synthesized Lead Zirconate Titanate Powders and Ceramics
Author 
Suwimon Nualpralaksana and Sukon Phanichphant*
Email 
psukon@yahoo.com
Abstract:
Fine powders of lead zirconate titanate [Pb(Zr0.52Ti0.48)O3, PZT] were prepared via a nitrate route by coprecipitation and freeze-drying processes. Lead nitrate, zirconium n-propoxide and titanium isopropoxide were used as starting materials. Ammonia solution, nitric acid and hydrogen peroxide were used to optimize the conditions for the preparation of PZT. The dried powders were calcined and characterized by thermogravimetric analysis (TGA), X-ray diffractometry (XRD) and scanning electron microscopy (SEM) techniques. Gravimetric analysis and atomic absorption spectrophotometry were performed. Perovskite PZT can be obtained at temperatures above 600 °C. PZT powders were pressed and sintered. XRD and SEM were used to characterized PZT ceramics.
Start & End Page 
129 - 140
Received Date 
2002-09-20
Revised Date 
Accepted Date 
2002-11-08
Full Text 
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Keyword 
lead zirconate titanate, coprecipitation process
Volume 
Vol.29 No.3 (DECEMBER 2002)
DOI 
Citation 
Nualpralaksana S. and Phanichphant S., Characterization of Nitrate Route Synthesized Lead Zirconate Titanate Powders and Ceramics, Chiang Mai J. Sci., 2002; 29(3): 129-140.
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Chiang Mai Journal of Science

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