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Comparison of Sizes, Morphologies and Optical Properties of NiO Nanostructures Synthesized Using Acetate and Nitrate Anions from Nickel Salts via Hydrothermal Method


Paper Type 
 Contributed Paper
Title 
 Comparison of Sizes, Morphologies and Optical Properties of NiO Nanostructures Synthesized Using Acetate and Nitrate Anions from Nickel Salts via Hydrothermal Method
Author 
 Pranwadee Kaewmuang, Watcharapong Pudkon, Anurak Prasatkhetragarn, Piyarat Nimmanpipug, Sila Kittiwachana, Sulawan Kaowphong*
Email 
 sulawank@gmail.com
Abstract:
Porous NiO nanocrystals were synthesized using a hydrothermal method in mediums of different anions from nickel salts, acetate (CH3COO-) and nitrate (NO3-),followed by calcination at 500 °C. Firstly, b-Ni(OH)2 powders with a hexagonal structure were formed. Using acetate and nitrate anions, the obtained b-Ni(OH)2 powders were composed of thin nanosheets (0.8-2.1 mm in length), and a splinter-like structure self-assembled with longer nanosheets (9.8-24.2 mm), respectively. The difference in the interaction ability between the anions and the b-Ni(OH)2 surfaces, affecting the growth behavior of the crystals, was examined using the density functional theory (DFT) method. After calcination, the b-Ni(OH)2 turned into porous NiO with a cubic structure but their morphologies were unchanged. The porous NiO with longer nanosheets possessing higher crystallinity and larger surface area provided better UV-Vis absorption ability.
Start & End Page 
 1122 - 1128
Received Date 
 2016-10-12
Revised Date 
Accepted Date 
 2016-12-29
Full Text 
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Keyword 
 NiO, Semiconductor, Nanocrystalline material, X-ray technique, Electron microscopy, Optical property
Volume 
 Vol.45 No.2 (March 2018)
DOI 
Citation 
 Kaewmuang P., Pudkon W., Prasatkhetragarn A., Nimmanpipug P., Kittiwachana S. and Kaowphong* S., Comparison of Sizes, Morphologies and Optical Properties of NiO Nanostructures Synthesized Using Acetate and Nitrate Anions from Nickel Salts via Hydrothermal Method, Chiang Mai Journal of Science, 2018; 45(2): 1122-1128.
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