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Characterization of CdS0.9Se0.1 Powder by Scanning Transmission Electron Microscopy


Paper Type 
Contributed Paper
Title 
Characterization of CdS0.9Se0.1 Powder by Scanning Transmission Electron Microscopy
Author 
Masahiro Kawasaki[a], Thanapat Autthawong[b], Thapanee Sarakonsri* [b,c], and Makoto Shiojiri[d,e]†
Email 
tsarakonsri@gmail.com
Abstract:
 n-type CdS0.9Se0.1 powder was produced by mixing and annealing of CdS and Se powders that were prepared by a reflux method using Cd(CH3CO)2 2H2O, thiourea and ethylene glycol, and by a solution method using SeO2, ethylene glycol and NaBH4, respectively. The product was supposed to be crystalline CdS0.9Se0.1 powder from simulation of X-ray diffraction pattern using CaRine 3.1 program and JCPDS card of CdS (space group P63mc). Analytical electron microscopy revealed that Cd, S and Se atoms were homogeneously distributed in the powder, which was composed of particles as fine as a few ten nm and in a single crystalline phase, supporting the formation of CdS0.9Se0.1. This CdS0.9Se0.1 powder is expected to be used as n-type thermoelectric materials.

 

Start & End Page 
282 - 287
Received Date 
2015-09-15
Revised Date 
Accepted Date 
2015-12-16
Full Text 
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Keyword 
electron microscopy, chalcogenides, semiconductor
Volume 
Vol.43 No.2 (SPECIAL ISSUE 1)
DOI 
SDGs
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