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Characterization of CdS0.9Se0.1 Powder by Scanning Transmission Electron Microscopy


Paper Type 
Contributed Paper
Title 
Characterization of CdS0.9Se0.1 Powder by Scanning Transmission Electron Microscopy
Author 
Masahiro Kawasaki[a], Thanapat Autthawong[b], Thapanee Sarakonsri* [b,c], and Makoto Shiojiri[d,e]†
Email 
tsarakonsri@gmail.com
Abstract:
 n-type CdS0.9Se0.1 powder was produced by mixing and annealing of CdS and Se powders that were prepared by a reflux method using Cd(CH3CO)2 2H2O, thiourea and ethylene glycol, and by a solution method using SeO2, ethylene glycol and NaBH4, respectively. The product was supposed to be crystalline CdS0.9Se0.1 powder from simulation of X-ray diffraction pattern using CaRine 3.1 program and JCPDS card of CdS (space group P63mc). Analytical electron microscopy revealed that Cd, S and Se atoms were homogeneously distributed in the powder, which was composed of particles as fine as a few ten nm and in a single crystalline phase, supporting the formation of CdS0.9Se0.1. This CdS0.9Se0.1 powder is expected to be used as n-type thermoelectric materials.

 

Start & End Page 
282 - 287
Received Date 
2015-09-15
Revised Date 
Accepted Date 
2015-12-16
Full Text 
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Keyword 
electron microscopy, chalcogenides, semiconductor
Volume 
Vol.43 No.2 (SPECIAL ISSUE 1)
DOI 
Citation 
Kawasaki M., Autthawong T., Sarakonsri T. and Shiojiri M., Characterization of CdS0.9Se0.1 Powder by Scanning Transmission Electron Microscopy , Chiang Mai J. Sci., 2016; 43(2): 282-287.
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