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Processing Parameters Study on Solution Route Synthesis of Dendrite Cu Sb Powders


Paper Type 
Contributed Paper
Title 
Processing Parameters Study on Solution Route Synthesis of Dendrite Cu Sb Powders
Author 
Thapanee Sarakonsri* [a], Thapakorn Aamchikad [a] and Tawee Tunkasiri [b]
Email 
scchi017@chiangmai.ac.th
Abstract:
Dendrite Cu2Sb powders, anode materials for lithium-ion batteries, were successfully synthesized by redox reaction between metal chloride salts and metallic reducing agent at ambient temperature. This experiment reports on the consequence of processing parameters, i.e. size of reducing agent particle and reaction temperature, to the formation of dendrite Cu2Sb powder. The results from XRD, SEM, and TEM techniques suggest that high purity dendrite Cu2Sb powder can be synthesized in ethylene glycol either by using zinc powder reducing agent having 10 µm particle size at any temperature or at 50°C reaction temperature with any reducing agent particle size.
Start & End Page 
321 - 326
Received Date 
2006-05-10
Revised Date 
Accepted Date 
2006-06-28
Full Text 
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Keyword 
copper antimonide, electron microscopy, intermetallic alloys and compounds, lithium-ion battery
Volume 
Vol.33 No.3 (SEPTEMBER 2006)
DOI 
Citation 
[a] T.S., [a] T.A. and [b] T.T., Processing Parameters Study on Solution Route Synthesis of Dendrite Cu Sb Powders, Chiang Mai Journal of Science, 2006; 33(3): 321-326.
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