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Extraction and Determination of Organochlorine and Carbamate Pesticides in Sediment Samples
Paper Type  |
Opinion |
Title |
Extraction and Determination of Organochlorine and Carbamate Pesticides in Sediment Samples |
Author |
Wanna Kanchanamayoon, Sirichai Hathongkam and Apirak Pongchamnong. |
Email |
- |
|
Abstract: Eight organochlorine pesticides in sediment were extracted twice, each with 20 ml diethylether for 30 min with the percentage recoveries in the ranges of 84.91-98.71. The detection limits for extraction of organochlorine in sediment were in the ranges of 0.32-0.90 ng/g. The soxhlet extraction was the method for removal of carbamate pesticides from sediment. The mixture of methanol–dichloromethane–acetone (1:1:1) was the suitable extracting solvent with the extraction time of 16 hours. The detection limits for extraction of carbamate pesticides in sediment were in the ranges of 2.1-3.1 ng/g. The results showed good percentage recoveries in the ranges of 81.35 - 96.49. These procedures were successfully applied to analysis of pesticides in 5 sediment samples.
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Start & End Page |
83 - 85 |
Received Date |
2000-12-12 |
Revised Date |
|
Accepted Date |
2001-08-27 |
Full Text |
Download |
Keyword |
gas chromatography, high performance liquid chromatography, soxhlet extraction |
Volume |
Vol.28 No.2 (DECEMBER 2001) |
DOI |
|
Citation |
Kanchanamayoon W., Hathongkam S. and Pongchamnong. A., Extraction and Determination of Organochlorine and Carbamate Pesticides in Sediment Samples , Chiang Mai Journal of Science, 2001; 28(2): 83-85. |
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