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Extraction and Determination of Organochlorine and Carbamate Pesticides in Sediment Samples


Paper Type 
Opinion
Title 
Extraction and Determination of Organochlorine and Carbamate Pesticides in Sediment Samples
Author 
Wanna Kanchanamayoon, Sirichai Hathongkam and Apirak Pongchamnong.
Email 
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Abstract:
Eight organochlorine pesticides in sediment were extracted twice, each with 20 ml diethylether for 30 min with the percentage recoveries in the ranges of 84.91-98.71. The detection limits for extraction of organochlorine in sediment were in the ranges of 0.32-0.90 ng/g. The soxhlet extraction was the method for removal of carbamate pesticides from sediment. The mixture of methanol–dichloromethane–acetone (1:1:1) was the suitable extracting solvent with the extraction time of 16 hours. The detection limits for extraction of carbamate pesticides in sediment were in the ranges of 2.1-3.1 ng/g. The results showed good percentage recoveries in the ranges of 81.35 - 96.49. These procedures were successfully applied to analysis of pesticides in 5 sediment samples.
Start & End Page 
83 - 85
Received Date 
2000-12-12
Revised Date 
Accepted Date 
2001-08-27
Full Text 
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Keyword 
gas chromatography, high performance liquid chromatography, soxhlet extraction
Volume 
Vol.28 No.2 (DECEMBER 2001)
DOI 
SDGs
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Chiang Mai Journal of Science

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