Chiang Mai Journal of Science

Print ISSN: 0125-2526 | eISSN : 2465-3845

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Extraction and Determination of Organochlorine and Carbamate Pesticides in Sediment Samples

Wanna Kanchanamayoon, Sirichai Hathongkam and Apirak Pongchamnong.
* Author for corresponding; e-mail address: -
Volume: Vol.28 No.2 (DECEMBER 2001)
Opinion
DOI:
Received: 12 December 2000, Revised: -, Accepted: 27 August 2001, Published: -

Citation: Kanchanamayoon W., Hathongkam S. and Pongchamnong. A., Extraction and Determination of Organochlorine and Carbamate Pesticides in Sediment Samples , Chiang Mai Journal of Science, 2001; 28(2): 83-85.

Abstract

Eight organochlorine pesticides in sediment were extracted twice, each with 20 ml diethylether for 30 min with the percentage recoveries in the ranges of 84.91-98.71. The detection limits for extraction of organochlorine in sediment were in the ranges of 0.32-0.90 ng/g. The soxhlet extraction was the method for removal of carbamate pesticides from sediment. The mixture of methanol–dichloromethane–acetone (1:1:1) was the suitable extracting solvent with the extraction time of 16 hours. The detection limits for extraction of carbamate pesticides in sediment were in the ranges of 2.1-3.1 ng/g. The results showed good percentage recoveries in the ranges of 81.35 - 96.49. These procedures were successfully applied to analysis of pesticides in 5 sediment samples.

Keywords: gas chromatography, high performance liquid chromatography, soxhlet extraction

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