Chiang Mai Journal of Science

Print ISSN: 0125-2526 | eISSN : 2465-3845

1,647
Articles
Q3 0.80
Impact Factor
Q3 1.3
CiteScore
7 days
Avg. First Decision

Disintegration Testing of Biodegradable Poly(L-lactide) / Thermoplastic Polyurethane Melt Blended Films

Kanyarat Suthapakti, Robert Molloy and Thanawadee Leejarkpai
* Author for corresponding; e-mail address: kanyarat.cmu@gmail.com
Volume: Vol.45 No.5 (Special 2018)
Research Article
DOI:
Received: 1 November 2017, Revised: -, Accepted: 30 April 2018, Published: -

Citation: Suthapakti K., Molloy R. and Leejarkpai T., Disintegration Testing of Biodegradable Poly(L-lactide) / Thermoplastic Polyurethane Melt Blended Films , Chiang Mai Journal of Science, 2018; 45(5): 2079-2091.

Abstract

Poly(L-lactide) (PLL) has been blended with a polycaprolactone-based thermoplastic polyurethane (TPU) elastomer as a toughening agent for potential use as a biodegradable film packaging material. The effects of adding a synthesized poly(L-lactide-co-caprolactone) (PLLCL) copolymer as a compatibilizer was also studied. Both 2-component (PLL/TPU) and 3-component (PLL/TPU/PLLCL) blends were prepared by melt mixing, hot-pressed into thin films and their compostability characterized in a standard ISO disintegration test under controlled laboratory-scale conditions. The results showed that both the 2- and 3-component blended film samples (25 ด 25 mm) disintegrated completely (100%) to fragments less than 2 mm in size within 30 days. These results were similar to those for PLL alone which indicated that neither the TPU nor the PLLCL had retarding effects on the PLL’s biodegradability. It is concluded that both the PLL/TPU and PLL/TPU/PLLCL blends meet the criteria for disintegration and compostability under simulated composting conditions.     

Keywords: Poly(L-lactide), thermoplastic polyurethane elastomer, poly(L-lactide-co-caprolactone, immiscible blend, disintegration test, compostability, biodegradable film

Related Articles

Poly(L-lactide)-Degrading Enzyme from Laceyella sacchari LP175: Cloning, Sequencing, Expression, Characterization and Its Hydrolysis of Poly(L-lactide) Polymer
page: 417 - 430

Thanasak Lomthong, Marie Guicherd, Gianluca Cioci, Sophie Duquesne, Alain Marty, Saisamorn Lumyong and Vichien Kitpreechavanich

Vol.46 No.3 (May 2019)
Research Article View: 1,074 Download: 488
Kinetics Studies of Non-Isothermal Melt Crystallization of Poly(ε-caprolactone) and Poly(L-lactide)
page: 329 - 338

Wanich Limwanich [a], Sawarot Phetsuk [b], Puttinan Meepowpan [b], Nawee Kungwan [b], Winita Punyodom*[b]

Vol.43 No.2 (SPECIAL ISSUE 1)
Research Article View: 996 Download: 323
Outline
Figures