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Simple Spectrophotometric Method for Determination of Iodine Value of Vegetable Oils


Paper Type 
Contributed Paper
Title 
Simple Spectrophotometric Method for Determination of Iodine Value of Vegetable Oils
Author 
Thidarat Kruatian [a] and Kritsana Jitmanee*[a,b,c]
Email 
kritsana.j@cmu.ac.th
Abstract:

A spectrophotometric method has been developed for the determination of iodine value of vegetable oils. The method is based on the reaction of Hanus solution with oils and subsequently treated with potassium iodide solution producing triiodide ions. The absorbance at 350 nm of triiodide ions was used for analytical purposes. The calibration graph was constructed by plotting the absorbance at 350 nm versus the molar concentration of Hanus solution. Under the optimal conditions a linear calibration graph ranged from 0.02 to 0.10 mol/L of Hanus solution with r

2 of 0.999. The proposed method was feasible to determine a wide range of iodine value of vegetable oil samples. The method was applied to commercially available vegetable oils and the results obtained by the proposed method agreed well with those obtained by the reference method. The standard deviation of iodine value ranged from 0.7 to 2.1 (n=3). The analytical procedures were simple, required short analysis time, and used small amount of solvent and reagent.
Start & End Page 
419 - 426
Received Date 
2012-04-10
Revised Date 
Accepted Date 
2012-06-26
Full Text 
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Keyword 
spectrophotometry, iodine value, vegetable oils
Volume 
Vol.40 No.3 (JULY 2013)
DOI 
Citation 
Kruatian T. and Jitmanee K., Simple Spectrophotometric Method for Determination of Iodine Value of Vegetable Oils, Chiang Mai J. Sci., 2013; 40(3): 419-426.
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Chiang Mai Journal of Science

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