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Synthesis and Characterization of β-Tricalcium Phosphate and Its Film Coating on a Ti6Al4V Metallic Biomaterial


Paper Type 
Contributed Paper
Title 
Synthesis and Characterization of β-Tricalcium Phosphate and Its Film Coating on a Ti6Al4V Metallic Biomaterial
Author 
Waraporn Boontakam, Kamonporn Saenkam, Phanrawee Sriprapha, Komsanti Chokethawai, Chamnan Randorn, Nopakarn Chandet, Kriangkrai Thongkorn, Tawee Tunkasiri and Gobwute Rujijanagul
Email 
rujijanagul@yahoo.com
Abstract:

     In the present work, the characteristic of β-tricalcium phosphate (β-TCP) powder was investigated for its film coating on a Ti6Al4V metallic biomaterial. The β-TCP powder was synthesized by a solid-state reaction technique at different temperatures. The β-TCP formed at temperatures 900-1000 oC, while α-tricalcium phosphate (α-TCP) was occurred at higher temperatures (≥1000 oC). Crystallite size increased with increasing temperature, but it decreased at temperatures higher than 1000 oC due to the formation of α-TCP. Furthermore, the amount of α-TCP phase increased with temperature. However, maximum crystallite size and density values were found for the 1000 oC powder. The 1000 oC powder was coated on a titanium alloy (Ti6Al4V) by a dip coating technique. The coated surface presented a uniform grain with an average grain size of 3.21 μm. Bioactivity testing of the coated samples indicated that they had good bioactivity. The results indicate the possibility of developing the samples for biomedical applications.

Article ID
e2024086
Received Date 
2024-05-20
Revised Date 
2024-08-13
Accepted Date 
2024-09-06
Keyword 
biomaterials, film coating, β-tricalcium phosphate, bioactivity
Volume 
Vol.51 No.6 In progress (November 2024). This issue is in progress but contains articles that are final and fully citable.
DOI 
https://doi.org/10.12982/CMJS.2024.086
Citation 
Boontakam W., Saenkam K., Sriprapha P., Chokethawai K., Randorn C., Chandet N., et al., Synthesis and Characterization of β-Tricalcium Phosphate and Its Film Coating on a Ti6Al4V Metallic Biomaterial, Chiang Mai J. Sci., 2024; 51(6): e2024086. DOI 10.12982/CMJS.2024.086.
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