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Efficient Solvent-free Synthesis of 14 H-Dibenzo[a,j] xanthenes Catalyzed by 2-Hydroxy-5-sulfobenzoic Acid


Paper Type 
Contributed Paper
Title 
Efficient Solvent-free Synthesis of 14 H-Dibenzo[a,j] xanthenes Catalyzed by 2-Hydroxy-5-sulfobenzoic Acid
Author 
Hamzeh Kiyani* and Hassan Darbandi
Email 
hkiyani@du.ac.ir
Abstract:
The use of 2-hydroxy-5-sulfobenzoic acid (2-HSBA) to demonstrate the catalyze one-pot condensation of 2-naphthol with various aldehydes under solvent-free conditions is described. This method can be implemented with a wide variety of readily accessible reagents to provide 14H-dibenzo[a,j]xanthenes as the dye candidates. A significant feature for the present method to the synthesis of 14H-dibenzo[a,j]xanthenes is that the reactions were performed in the absence of solvent and give products in good to high yields. This approach is reasonably priced, and commercially available of the catalyst is also valuable point for the presented procedure. 
Start & End Page 
1504 - 1511
Received Date 
2016-01-16
Revised Date 
Accepted Date 
2016-03-24
Full Text 
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Keyword 
2-hydroxy-5-sulfobenzoic acid, 2-naphthol, 14H-dibenzo[a,j]xanthene, solvent-free, condensation
Volume 
Vol.44 No.4 (October 2017)
DOI 
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