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Synthesis of Nanosized Anatase Particles from Commercial Rutile Powder by Using Hydrothermal Method


Paper Type 
Contributed Paper
Title 
Synthesis of Nanosized Anatase Particles from Commercial Rutile Powder by Using Hydrothermal Method
Author 
Ubonwan Chutiphunphinyo, Siriporn Larpkiattaworn and Pornapa Sujaridworakun
Email 
pornapa.s@chula.ac.th
Abstract:
Nanosized anatase particles with size ranging from 5.73 nm to 8.26 nm were prepared by low temperature hydrothermal process (150C) using commercial rutile powder as a starting material. Various parameters such as pH, hydrothermal temperature and reaction time were studied. It was found that, the degree of  crystallinity, crystallite size, and specific surface area of anatase powder can be controlled by varying these parameters. The synthesized powders were characterized by XRD, SEM, BET and UV-VIS spectrophotometer.  The results show that pH value affected obviously on the photocatalytic activity of anatase.  The anatase obtained under pH7, hydrothermal at 150C for 6h has crystallite size about 8.26 nm and specific surface area 164.87 m2/g which its photocatalytic activity closes to that of commercial photocatalyst (ST-01)
Start & End Page 
1 - 5
Received Date 
2007-09-20
Revised Date 
Accepted Date 
2007-10-15
Full Text 
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Keyword 
Nanosized, anatase, rutile, hydrothermal
Volume 
Vol.35 No.1 (JANUARY 2008)
DOI 
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Chiang Mai Journal of Science

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